CuAAC "click'' active-template synthesis of functionalised [2] rotaxanes using small exo-substituted macrocycles: how small is too small?

Asif Noor; Warrick K. C. Lo; Stephen C. Moratti; James D. Crowley

doi:10.1039/c4cc03077j

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CuAAC "click'' active-template synthesis of functionalised [2] rotaxanes using small exo-substituted macrocycles: how small is too small?

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CuAAC "click'' active-template synthesis of functionalised [2] rotaxanes using small exo-substituted macrocycles: how small is too small?

Asif Noor, Warrick K. C. Lo, Stephen C. Moratti and James D. Crowley

Chemical communications (Cambridge, England), Vol.50(53), pp.7044-7047

01/01/2014

DOI: https://doi.org/10.1039/c4cc03077j

Abstract

Chemistry

Chemistry, Multidisciplinary

Physical Sciences

Science & Technology

Two "small'' 22- and 24-membered exo-alcohol functionalised pyridyl macrocycles are exploited in the CuAAC active-template synthesis of [2] rotaxanes. The 24-membered macrocycle forms [2] rotaxanes in good yields while the smaller 22-membered macrocycle does not lead to interlocked products.

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Record Identifier: 9926516778901891
Title: CuAAC "click'' active-template synthesis of functionalised [2] rotaxanes using small exo-substituted macrocycles: how small is too small?
Creators: Asif Noor
Warrick K. C. Lo
Stephen C. Moratti
James D. Crowley
Publication Details: Chemical communications (Cambridge, England), Vol.50(53), pp.7044-7047
Academic Unit: Chemistry
Publisher: Royal Soc Chemistry
Grant note: UOOX1206 / NZ Ministry of Business, Innovation and Employment Science Investment Fund; New Zealand Ministry of Business, Innovation and Employment (MBIE) Department of Chemistry, University of Otago University of Otago
Date published ; e-published: 01/01/2014
Language: English
Resource Type: Journal article

CuAAC "click'' active-template synthesis of functionalised [2] rotaxanes using small exo-substituted macrocycles: how small is too small?

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